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Beilstein J. Org. Chem. 2015, 11, 659–667, doi:10.3762/bjoc.11.74
Graphical Abstract
Figure 1: N-Bu DNJ (1) and examples of potent multivalent pharmacological chaperones and CFTR correctors (2 a...
Figure 2: Azide-armed DNJ derivatives 4 and polyalkyne “clickable” scaffolds 5 and 6.
Scheme 1: Synthesis of trisubstituted BODIPY derivatives. (a) ICl, CHCl3/MeOH, rt, 15 min, quantitative; (b) ...
Scheme 2: Synthesis of DNJ clusters 13: (a) CuSO4·5H2O cat., sodium ascorbate, THF/H2O (1:1), 83% (12a), 56% (...
Scheme 3: Synthesis of DNJ clusters 15: (a) CuSO4·5H2O cat., sodium ascorbate, DMF/H2O (6:1), 80 °C (MW) or r...
Figure 3: a) Absorption (orange line), corrected emission (green line) (λexc = 510 nm), excitation (dashed bl...
Figure 4: a) Absorption (orange line), corrected emission (green line) (λexc = 360 nm) and excitation (dashed...
Beilstein J. Org. Chem. 2014, 10, 1406–1412, doi:10.3762/bjoc.10.144
Figure 1: N-Bu-DNJ (1), azide-armed DNJ derivatives 5 and cyclopeptoid scaffolds 2–4.
Scheme 1: Sub-monomer approach for the synthesis of cyclopeptoids 2–4: DIPEA = N,N-diisopropylethylamine; DIC...
Scheme 2: Synthesis of DNJ clusters 10: (a) CuSO4·5H2O cat., sodium ascorbate, DMF/H2O (5:1), MW, 80 °C; (b) ...
Figure 2: i) Partial 1H NMR spectrum (400 MHz, CD3CN/CDCl3 9:1) of compound 9a; ii) Partial 1H NMR spectrum (...
Figure 3: Monovalent models 11 and 7-valent DNJ derivatives 12.